HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → tert-Butyl 4-(2-methoxy-2-oxoethyl)piperidine-1-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | Tert-butyl 4-(2-methoxy-2-oxoethylidene)piperidine-1-carboxylate | HCID 10377658 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | tert-Butyl 4-(2-methoxy-2-oxoethyl)piperidine-1-carboxylate | HCID 1514280 | 99,9% |
Reaktionsschritte
tert-Butyl 4-(2-methoxy-2-oxoethylidene)piperidine-1-carboxylate (3.6 g, 14 mmol) and 10% Pd/C moistered with water (0.8 g) was mixed in MeOH (75 mL) and stirred under H2 (1 atm) for 4 h. The mixture was filtered through Celite and concentrated to give the title compound (3.6 g, 99%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07427631B2 |
| Quelldatensatz | uspto-grants-2008_09 |
| ORD ID | ord-48d486ba3dc64acaae68325a2655a90a |
| Quellennotiz | uspto-grants-2008_09 |