HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Hexene → 5-Decenoic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Hexene | HCID 11597 | — |
| Edukt | 5-Hexenoic Acid | HCID 15308 | — |
| Edukt | Dec-5-enyl acetate | HCID 38027 | — |
| Katalysator | HCID 178479819 | HCID 178479819 | — |
| Produkt | 5-Decenoic acid | HCID 53400879 | — |
Reaktionsschritte
FIG. 6 shows an alternative synthesis of 5-decenyl acetate, in which 1-hexene is reacted with 5-hexenoic acid in the presence of Grubbs' catalyst to produce 5-decenoic acid that can be recrystallized, reduced to an alcohol, and acetylated to yield a greater than 90% E-5-decenyl acetate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06215019B1 |
| Quelldatensatz | uspto-grants-2001_04 |
| ORD ID | ord-adf99e6f273840459f17678167ea6b71 |
| Quellennotiz | uspto-grants-2001_04 |