HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → Acridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Isatin | HCID 7054 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Lösungsmittel | Potassium Hydroxide | HCID 14797 | — |
| Produkt | Acridine | HCID 9215 | — |
Reaktionsschritte
The isatin product was refluxed in 110 mL of 10% KOH solution in water over night. The dark green mixture was cooled and acidified with 400 mL of 1:1 ice/5 M HCl. The solid was washed with water and air-dried yielding the acridine acid. 1H NMR (DMSO-d6) δ 7.81-7.94 (m, 4H), 8.31-8.36 (m, 2H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06218137B1 |
| Quelldatensatz | uspto-grants-2001_04 |
| ORD ID | ord-899d982ee2cd4e77a93c91ee5f87c025 |
| Quellennotiz | uspto-grants-2001_04 |