3-Thiophen-2-ylprop-2-enoic acid → 3-(2-Thienyl)propanoic acid

Beteiligte Stoffe

Reaktionsschritte

To a solution of 3-(2-thienyl)acrylic acid (7 g) in ethanol was added 5% palladium on carbon and the mixture was hydrogenated at 50 psi in a Parr apparatus. The catalyst was filtered off and the solvent was removed by evaporation to yield the title compound (5.5 g) as an oil. Electrospray MS m/z 155 [M−H]+.

Herkunft & Nachweise