Ammonia → n-Octadecenyl-succinic monoamide

Reaktionsgleichung

[NH3:1].[CH:2]([CH:20]1[CH2:25][C:24](=[O:26])[O:23][C:21]1=[O:22])=[CH:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].Cl>C(#N)C>[CH:2]([CH:20]([CH2:25][C:24]([OH:23])=[O:26])[C:21]([NH2:1])=[O:22])=[CH:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Komponenten

Versuchsvorschrift

389 g of a 25% aqueous ammonia was mixed with 200 ml of acetonitrile and to the mixture was added 100 g of n-octadecenylsuccinic anhydride, followed by stirring for 2 hours at room temperature. The mixture was neutralized with concentrated hydrochloric acid. The crystals thus-deposited were collected by filtration, washed with water and then with acetonitrile, and dried to obtain 84.5 g of n-octadecenyl-succinic monoamide as colorless crystals.