HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
alpha-Tocopherol → HCID 86756642, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | alpha-Tocopherol | HCID 14985 | — |
| Edukt | Benzoyl chloride, 4-amino- | HCID 177720 | — |
| Katalysator | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | HCID 86756642 | HCID 86756642 | 68% |
Reaktionsschritte
The reaction of alpha-tocopherol with 4-aminobenzoic acid chloride was carried out in the same manner with Example I, except that 10 mol % of 4-(dimethylamino)pyridine was added together with pyridine. This reaction was confirmed to proceed in a similar pattern to that of Example I as measured by thin layer chromatography. The remaining processes of Example I were repeated to produce alpha-tocopherol 4-aminobenzoate (0.61 g, yield 68%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06222051B1 |
| Quelldatensatz | uspto-grants-2001_04 |
| ORD ID | ord-84a2330b294a46d5b04e558ac57f83de |
| Quellennotiz | uspto-grants-2001_04 |