HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromopentadecane → 3-Pentadecylthiopropanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromopentadecane | HCID 12394 | — |
| Edukt | Ethyl 3-mercaptopropionate | HCID 21625 | — |
| Edukt | Aluminium lithium hydride | HCID 21226445 | — |
| Produkt | 3-Pentadecylthiopropanol | HCID 20462062 | 84% |
Reaktionsschritte
1-Bromopentadecane is reacted in the usual way with ethyl β-mercaptopropionate and the syrup obtained reduced with lithium aluminium hydride to give a yield of 84% of theory of 3-pentadecylthiopropanol; m.p. 36°-39° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04444766 |
| Quelldatensatz | uspto-grants-1984_04 |
| ORD ID | ord-b31fba29f7574ee6a1a36ee713ddad8d |
| Quellennotiz | uspto-grants-1984_04 |