HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,2,6,6-Tetramethyl-4-piperidone → N-(2,2,6,6-tetramethyl-4-piperidyl)-3-morpholinopropylamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,2,6,6-Tetramethyl-4-piperidone | HCID 13220 | — |
| Edukt | N-(3-Aminopropyl)morpholine | HCID 61055 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | N-(2,2,6,6-tetramethyl-4-piperidyl)-3-morpholinopropylamine | HCID 19736767 | — |
Reaktionsschritte
288.4 g (2 mol) of 3-morpholinopropylamine, 310.5 g (2 mol) of 2,2,6,6-tetramethyl-4-piperidone and 300 ml of methanol are introduced into a 2 litre autoclave; 15 g of 5% Pt-on-carbon are added, and hydrogenation is carried out at 60 bar and 60° C. until the absorption of hydrogen ceases (about 15 hours).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05268401 |
| Quelldatensatz | uspto-grants-1993_12 |
| ORD ID | ord-da77c7797a634342bdc5c8cedae7aaa1 |
| Quellennotiz | uspto-grants-1993_12 |