Sodium Hydroxide → HCID 23718315, Verbindung

HRID 326786Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 326786
[CH2:1]([CH:3]([CH2:13][CH3:14])[C:4]([NH:6][CH2:7][C:8]([O:10]CC)=[O:9])=[O:5])[CH3:2].[OH-].[Na+:16]>CO>[CH2:13]([CH:3]([CH2:1][CH3:2])[C:4]([NH:6][CH2:7][C:8]([O-:10])=[O:9])=[O:5])[CH3:14].[Na+:16]

Komponenten

4

Edukt 2

HCID 14798Sodium HydroxideHCID 2268387Ethyl 2-(2-ethylbutanoylamino)acetate

Produkt 1

HCID 23718315HCID 23718315, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

To a solution of ethyl N-(2-ethylbutyryl)glycinate (33.73 g) in 100 mL of methanol was added 167.6 mL of 1N sodium hydroxide, and the solution stirred for 1.5 hr. Solvents were evaporated in vacuo, and then fresh methanol was added and evaporated to give 32.6 g of a pale yellow oil.

Aufarbeitung

  1. customSolvents were evaporated in vacuo
  2. additionfresh methanol was added
  3. customevaporated

Quellen und Nachweise

ORD-Eintrag
ord-4e69deb7f80a40ca802f059a16d2cd57
Quelldatensatz
uspto-grants-1993_12
Patentnummer
US05270331

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