Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Calcium Acetate | HCID 6116 | — |
| Edukt | 3-(1-Dodecen-1-yl)dihydro-2,5-furandione | HCID 32933 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Lösungsmittel | Isopropanol | HCID 3776 | — |
| Produkt | Calcium dodecenyl succinate | HCID 86747412 | 113,2% |
Reaktionsschritte
A solution of 313.5 g (1.98 mol) calcium acetate in 1000 ml water was added to a solution of 570 g (1.98 mol) dodecenyl succinic anhydride in 1000 ml isopropanol. The mixture was then heated to 90° C., left at that temperature for 1.5 h and then concentrated in a water jet vacuum. The residue was dried in vacuo in a drying cabinet at 100° C. 680 g of the calcium soap were obtained in the form of a colorless powder.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05271855 |
|---|
| Quelldatensatz | uspto-grants-1993_12 |
|---|
| ORD ID | ord-93f2ffbeba514eb389fbfa7f33845a47 |
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| Quellennotiz | uspto-grants-1993_12 |
|---|
