4-Amino-1-methyl-3-propyl-1H-pyrazole-5-carboxamide → 4-(5-Acetyl-2-ethoxybenzamido)-1-methyl-3-n-propylpyrazole-5-carboxamide

HRID 327071

Reaktionsgleichung

Reaktionsgleichung von HRID 327071
[C:1]([C:4]1[CH:5]=[CH:6][C:7]([O:13][CH2:14][CH3:15])=[C:8]([CH:12]=1)[C:9](Cl)=[O:10])(=[O:3])[CH3:2].[NH2:16][C:17]1[C:18]([CH2:26][CH2:27][CH3:28])=[N:19][N:20]([CH3:25])[C:21]=1[C:22]([NH2:24])=[O:23]>>[C:1]([C:4]1[CH:5]=[CH:6][C:7]([O:13][CH2:14][CH3:15])=[C:8]([CH:12]=1)[C:9]([NH:16][C:17]1[C:18]([CH2:26][CH2:27][CH3:28])=[N:19][N:20]([CH3:25])[C:21]=1[C:22]([NH2:24])=[O:23])=[O:10])(=[O:3])[CH3:2]

Komponenten

3

Edukt 2

HCID 33380444-Amino-1-methyl-3-propyl-1H-pyrazole-5-carboxamideHCID 212508125-Acetyl-2-ethoxybenzoyl chloride

Produkt 1

HCID 539584074-(5-Acetyl-2-ethoxybenzamido)-1-methyl-3-n-propylpyrazole-5-carboxamide

Versuchsvorschrift

The title compound was prepared form 5-acetyl-2-ethoxybenzoyl chloride and 4-amino-1-methyl-3-n-propylpyrazole-5-carboxamide following the procedure of Preparation 6, and was obtained as a white solid (60%), m.p. 225°-227° C. Found: C,61.35; H,6.25; N,15.07. C19H24N4O4 requires C,61.28; H,6.50; N,15.04%

Aufarbeitung

  1. customthe procedure of Preparation 6

Quellen und Nachweise

ORD-Eintrag
ord-9128faef0ac1461897886d2ec28e000e
Quelldatensatz
uspto-grants-1993_12
Patentnummer
US05272147

Verknüpfte Notizen

Wird geladen…