2-Phenoxy-1-propanol → 2-Phenoxypropanol sulfamate

HRID 327674

Reaktionsgleichung

Reaktionsgleichung von HRID 327674
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[O:6]([CH:13]([CH3:16])[CH2:14][OH:15])[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1>>[S:1]([O:15][CH2:14][CH:13]([O:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH3:16])(=[O:4])(=[O:3])[NH2:2]

Komponenten

3

Edukt 2

HCID 201292-Phenoxy-1-propanolHCID 24499Chlorosulfamic acid

Produkt 1

HCID 191086852-Phenoxypropanol sulfamate

Versuchsvorschrift

The title compound was prepared by procedures of Example 33 from sulfamoyl chloride and 2-phenoxypropanol. The oil obtained was further purified as in Example 38 by chromatography and recrystallization to give the title compound as colorless, viscous oil in 35% yield.

Aufarbeitung

  1. customThe oil obtained
  2. customwas further purified as in Example 38 by chromatography and recrystallization

Quellen und Nachweise

ORD-Eintrag
ord-c542b5daa73348c2ae7beeb85446aba1
Quelldatensatz
uspto-grants-1993_12
Patentnummer
US05273993

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