HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-Bromopentyl acetate → (E)-3-[2-[[5-(Acetyloxy)pentyl]oxy]-6-(6-hydroxy-1-hexynyl)phenyl]-2-propenoic Acid Methyl Ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-Bromopentyl acetate | HCID 85140 | — |
| Edukt | (E)-3-[2-Hydroxy-6-(6-hydroxy-1-hexynyl)phenyl]-2-propenoic Acid Methyl Ester | HCID 67780365 | — |
| Produkt | (E)-3-[2-[[5-(Acetyloxy)pentyl]oxy]-6-(6-hydroxy-1-hexynyl)phenyl]-2-propenoic Acid Methyl Ester | HCID 67780134 | 77% |
Reaktionsschritte
Using the procedure of example 63, (E)-3-[2-hydroxy-6-(6-hydroxy-1-hexynyl)phenyl]-2-propenoic acid methyl ester from the preceding example was converted into the title compound by alkylation with 5-bromopentylacetate. The product was obtained as a colorless oil in 77% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05273999 |
| Quelldatensatz | uspto-grants-1993_12 |
| ORD ID | ord-03d2ce19dc984a52b0d1775b100668d0 |
| Quellennotiz | uspto-grants-1993_12 |