Dodecanoyl chloride → 2-[Benzoyl(2-dodecanoyloxyethyl)amino]ethyl dodecanoate

HRID 328428

Reaktionsgleichung

Reaktionsgleichung von HRID 328428
[OH:1][CH2:2][CH2:3][N:4]([CH2:13][CH2:14][OH:15])[C:5](=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1.[C:16](Cl)(=[O:28])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27]>>[C:16]([O:1][CH2:2][CH2:3][N:4]([CH2:13][CH2:14][O:15][C:16](=[O:28])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27])[C:5](=[O:12])[C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][CH:11]=1)(=[O:28])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27]

Komponenten

3

Edukt 2

HCID 8166Dodecanoyl chlorideHCID 94109N,N-Bis(2-hydroxyethyl)benzamide

Produkt 1

HCID 3216882-[Benzoyl(2-dodecanoyloxyethyl)amino]ethyl dodecanoate

Versuchsvorschrift

N,N-bis(2-lauroyloxyethyl)-benzamide was prepared by the procedure of example 1 from 19.5 gms. (0.1 mole) of N,N-bis(2-hydroxyethyl)benzamide and 44 gms. (0.2 mole) of lauroyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Aufarbeitung

  1. customN,N-bis(2-lauroyloxyethyl)-benzamide was prepared by the procedure of example 1 from 19.5 gms

Quellen und Nachweise

ORD-Eintrag
ord-ae27b68bebe9463b9370f4c75862162b
Quelldatensatz
uspto-grants-1977_04
Patentnummer
US04017522

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