N,N-Bis(2-hydroxyethyl)benzamide → N,N-bis(2-erucoyloxyethyl)benzamide

HRID 328430

Reaktionsgleichung

Reaktionsgleichung von HRID 328430
[OH:1][CH2:2][CH2:3][N:4]([CH2:13][CH2:14][OH:15])[C:5](=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1.[C:16](Cl)(=[O:38])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27]/[CH:28]=[CH:29]\[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37]>>[C:16]([O:1][CH2:2][CH2:3][N:4]([CH2:13][CH2:14][O:15][C:16](=[O:38])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27]/[CH:28]=[CH:29]\[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37])[C:5](=[O:12])[C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][CH:11]=1)(=[O:38])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27]/[CH:28]=[CH:29]\[CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH3:37]

Komponenten

3

Edukt 2

HCID 94109N,N-Bis(2-hydroxyethyl)benzamideHCID 5364502Erucoyl chloride

Produkt 1

HCID 54598631N,N-bis(2-erucoyloxyethyl)benzamide

Versuchsvorschrift

N,N-bis(2-erucoyloxyethyl)benzamid was prepared by the procedure of example 1 from 19.5 gms. (0.1 mole) of N,N-bis(2-hydroxyethyl)benzamide and 71 gms. (0.2 mole) of erucoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Aufarbeitung

  1. customN,N-bis(2-erucoyloxyethyl)benzamid was prepared by the procedure of example 1 from 19.5 gms

Quellen und Nachweise

ORD-Eintrag
ord-7c54b5e1adc2457296b177b2a1af74e6
Quelldatensatz
uspto-grants-1977_04
Patentnummer
US04017522

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