Dodecanoyl chloride → 2-[Methyl(4-methylbenzoyl)amino]ethyl dodecanoate

HRID 328443

Reaktionsgleichung

Reaktionsgleichung von HRID 328443
[CH3:1][N:2]([CH2:12][CH2:13][OH:14])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4].[C:15](Cl)(=[O:27])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>>[CH3:1][N:2]([CH2:12][CH2:13][O:14][C:15](=[O:27])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4]

Komponenten

3

Edukt 2

HCID 8166Dodecanoyl chlorideHCID 21441887N-(2-hydroxyethyl)-N,4-dimethylbenzamide

Produkt 1

HCID 214418812-[Methyl(4-methylbenzoyl)amino]ethyl dodecanoate

Versuchsvorschrift

N-methyl-N-(2-lauroyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)-p-toluamide and 22 gms. (0.1 mole) of lauroyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Aufarbeitung

  1. customN-methyl-N-(2-lauroyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms

Quellen und Nachweise

ORD-Eintrag
ord-18cfc6ff3a2249b884f95b49c1629176
Quelldatensatz
uspto-grants-1977_04
Patentnummer
US04017522

Verknüpfte Notizen

Wird geladen…