Oleoyl chloride → N-methyl-N-(2-oleoyloxyethyl)-p-toluamide

HRID 328444

Reaktionsgleichung

Reaktionsgleichung von HRID 328444
[CH3:1][N:2]([CH2:12][CH2:13][OH:14])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4].[C:15](Cl)(=[O:33])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]/[CH:23]=[CH:24]\[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32]>>[CH3:1][N:2]([CH2:12][CH2:13][O:14][C:15](=[O:33])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]/[CH:23]=[CH:24]\[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4]

Komponenten

3

Edukt 2

HCID 5364783Oleoyl chlorideHCID 21441887N-(2-hydroxyethyl)-N,4-dimethylbenzamide

Produkt 1

HCID 68123309N-methyl-N-(2-oleoyloxyethyl)-p-toluamide

Versuchsvorschrift

N-methyl-N-(2-oleoyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)-p-toluamide and 30 gms. (0.1 mole) of oleoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

Aufarbeitung

  1. customN-methyl-N-(2-oleoyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms

Quellen und Nachweise

ORD-Eintrag
ord-af13e5383dc24d6e8fc9b3614a7f2665
Quelldatensatz
uspto-grants-1977_04
Patentnummer
US04017522

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