Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Glycine | HCID 750 | — |
| Edukt | Nitrate | HCID 943 | — |
| Edukt | Magnesium Carbonate | HCID 11029 | — |
| Edukt | Aluminum Sulfate | HCID 24850 | — |
| Edukt | Aluminum Hydroxide | HCID 10176082 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Magnesium Glycinate | HCID 84645 | — |
Reaktionsschritte
Magnesium glycinate was prepared by reacting 5 grams of glycine with 3.1 grams of basic magnesium carbonate (26.3% Mg) in 15 grams of water. The mixture was heated at 75° C. for 1/2 hour with agitation. The hot solution was then added to 113 grams of zirconyl nitrate (7.9% Zr) with stirring. After the addition of 1.5 grams of aluminum hydroxide powder (28.8% Al), the mixture was reacted with agitation at 75° C. for 1/2 hour. To the resultant clear solution was added 7.9 grams of 2/3 basic aluminum sulfate, Al(OH)2SO4 (3.1% Al). The solution was then oven dried at 58° C. under a vacuum of 328 mm of Hg. The product contained 1.2% Mg, 13.2% glycine, 1.5% Al, 24.3% Zr, 4.02% SO4 and 29.5% nitrate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US04017599 |
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| Quelldatensatz | uspto-grants-1977_04 |
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| ORD ID | ord-b20a6d4cdab24044b85bc4f29bad8363 |
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| Quellennotiz | uspto-grants-1977_04 |
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