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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 328905Erstellt: 25. Oktober 2026

Isopropylamine → 1-(Iso-propyl)-3-benzyloxyazetidine

https://huagongshe.com/reaction/328905

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktIsopropylamineHCID 6363—
Edukt(((1,3-Dibromopropan-2-yl)oxy)methyl)benzeneHCID 561824—
LösungsmittelWaterHCID 962—
Produkt1-(Iso-propyl)-3-benzyloxyazetidineHCID 20517324—

Reaktionsbedingungen

Temperatur80 °C

Reaktionsschritte

11 parts of 2-benzyloxy-1,3-dibromo-propane, 30 parts of iso-propylamine and 30 parts of water were added to a stainless autoclave, and the mixture was heated at 80° C. for 2 hours with agitation. The reaction mixture was cooled and treted in the same manner as in Example 29, followed by distillation under reduced pressure. As a result 18 parts of 3-benzyloxy-1-(iso-propyl)azetidine boiling at 104° - 107° C. under 2 mm Hg were obtained

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04018824
Quelldatensatzuspto-grants-1977_04
ORD IDord-330dfd270f7d46279404f665951ed1bd
Quellennotizuspto-grants-1977_04