HCID 21440130, Verbindung → HCID 21440219, Verbindung
Reaktionsgleichung
[C:1]([C:9]1[C:17]([N+:18]([O-])=O)=[CH:16][C:12]([C:13]([OH:15])=[O:14])=[CH:11][C:10]=1[O:21][CH2:22][CH2:23][CH2:24]C)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(OC1C=C(C=C([N+]([O-])=O)C=1C(=O)C1C=CC=CC=1)C(O)=O)C=C>>[CH2:22]([O:21][C:10]1[CH:11]=[C:12]([CH:16]=[C:17]([NH2:18])[C:9]=1[C:1](=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)[C:13]([OH:15])=[O:14])[CH:23]=[CH2:24]Komponenten
3
Versuchsvorschrift
By replacing in Example 1, step C, 4-benzoyl-3-n-butoxy-5-nitrobenzoic acid with 3-allyloxy-4-benzoyl-5-nitrobenzoic acid, and following the procedure described, 3-allyloxy-5-amino-4-benzoylbenzoic acid is obtained with a melting point of 206.5°-207.5° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-8d72c98d092c45abb321ba8ebf584cf3
- Quelldatensatz
- uspto-grants-1977_04
- Patentnummer
- US04018794