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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 329042Erstellt: 25. Oktober 2026

Benzoyl chloride, 3,4,5-trimethoxy- → 2-Trifluoromethyl-10-[3{4-[2-(3,4,5-trimethoxy-benzoyloxy)-ethoxy]-piperidino}-propyl]-phenothiazine

https://huagongshe.com/reaction/329042

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktBenzoyl chloride, 3,4,5-trimethoxy-HCID 78282—
EduktFlupimazineHCID 218089—
Produkt2-Trifluoromethyl-10-[3{4-[2-(3,4,5-trimethoxy-benzoyloxy)-ethoxy]-piperidino}-propyl]-phenothiazineHCID 2144092733%

Reaktionsschritte

Using the procedure of Example XXXV, 18.7 g (0.04 mole) of 2-trifluoromethyl-10-[3-(4-β-hydroxyethoxy-piperidino)-propyl]-phenothiazine (prepared in Example XXIII) and 9.2 g (0.04 mole) of 3,4,5-trimethoxy-benzoyl chloride were reacted to obtain 8.5 g (33% yield) of 2-trifluoromethyl-10-[ 3{ 4-[2-(3,4,5-trimethoxy-benzoyloxy)-ethoxy]-piperidino}-propyl]-phenothiazine as a clear amber oil

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04018922
Quelldatensatzuspto-grants-1977_04
ORD IDord-590cbc7787f34e64aa1061e0abd7d3b1
Quellennotizuspto-grants-1977_04