Sodium → 2-(1-[2-naphthyl]ethylthio)pyridine N-oxide
Reaktionsgleichung
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH:11](Cl)[CH3:12].[SH:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][N+:16]=1[O-:21].[Na]>>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH:11]([S:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][N+:16]=1[O-:21])[CH3:12]Komponenten
4
Versuchsvorschrift
The intermediate 2-(1-[2-naphthyl]ethylthio)pyridine N-oxide is prepared from 1-(2-naphthyl)ethyl chloride and 2-mercapto pyridine N-oxide, sodium salt by the procedure described in Example 2. Melting point 112° - 115° C. Structure confirmed by IR and NMR.
Quellen und Nachweise
- ORD-Eintrag
- ord-c5a0d952931147249ffa2b81b9e72b14
- Quelldatensatz
- uspto-grants-1977_04
- Patentnummer
- US04019893
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