HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetyl chloride → 1-(3-acetyltetrahydro-2H-1,3-thiazin-2-ylidene)-3-(2,4-dichlorophenoxy)-1-nitro-2-propanone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetyl chloride | HCID 6367 | — |
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | 3-(2,4-dichlorophenoxy)-1-nitro-1-(tetrahydro-2H-1,3-thiazin-2-ylidene)-2-propanone | HCID 86734697 | — |
| Produkt | 1-(3-acetyltetrahydro-2H-1,3-thiazin-2-ylidene)-3-(2,4-dichlorophenoxy)-1-nitro-2-propanone | HCID 54572089 | — |
Reaktionsschritte
5 was prepared as a yellow solid, melting point: 120°-120.5° (with decomposition) by the treatment of 5C with sodium hydride and acetyl chloride, by the general procedure described in Example 1.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04020061 |
| Quelldatensatz | uspto-grants-1977_04 |
| ORD ID | ord-acccc7e676614654bd37998f8b414146 |
| Quellennotiz | uspto-grants-1977_04 |