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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 329287Erstellt: 25. Oktober 2026

Ethyl 3-oxovalerate → Diethyl 2-Propionylazelate

https://huagongshe.com/reaction/329287

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthyl 3-oxovalerateHCID 78656—
EduktEthyl 7-bromoheptanoateHCID 122490—
EduktMethyl 8-Ethoxycarbonyl-9-oxo-5-decynoateHCID 22759276—
ProduktDiethyl 2-PropionylazelateHCID 22759291—

Reaktionsschritte

The synthesis of this compound is carried out by the procedure of Example 4, Step A, except that an equivalent quantity of ethyl propionylacetate is substituted for the ethyl acetoacetate of Example 4, Step A, and an equivalent quantity of ethyl 7-bromoheptanoate is substituted for the methyl 7-bromo-5-heptynoate of Example 4, Step A. The product, a viscous oil, is used in the next step directly without distillation.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04020177
Quelldatensatzuspto-grants-1977_04
ORD IDord-1d04c4f7b26c455ab875a2cad5831cf3
Quellennotizuspto-grants-1977_04