17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3-one → 17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3beta-ol

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3-one	HCID 13020886	—
Edukt	Lithium tri-tert-butoxyaluminohydride	HCID 16710494	—
Produkt	17beta-Acetoxy-1alpha-methyl-17alpha-n-propyl-5alpha-androstan-3beta-ol	HCID 70360261	64,7%

Reaktionsschritte

1.0 g of 17β-acetoxy-1α-methyl-17α-n-propyl-5α-androstan-3-one is reacted as described in Example 6 with lithium tri-tert.-butoxyaluminum hydride and worked up. After chromatography on silica gel, 650 mg of 17β-acetoxy-1α-methyl-17α-n-propyl-5α-androstan-3β-ol is obtained as an oil.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US04892867
Quelldatensatz	uspto-grants-1990_01
ORD ID	ord-adeedd16207e4916ba3804d85c5050fb
Quellennotiz	uspto-grants-1990_01