HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Perchlorate → Phenylphosphine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Perchlorate | HCID 123351 | — |
| Edukt | 1-Methylphenylphosphanium carbonate | HCID 86743659 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Phenylphosphine | HCID 12519 | — |
| Produkt | Methylphosphanium perchlorate | HCID 19871530 | — |
Reaktionsschritte
By following the same procedure as the 2nd step of Example 12 except that 10.0 g of 1-methylphenylphosphanium carbonate, 6.9 g of 60% perchlorate, and 10.0 g of water were used, 10.9 g (94.8% of the theoretical yield, yield of 67.6% to 1-phenylphosphane) of methylphosphanium perchlorate was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04892944 |
| Quelldatensatz | uspto-grants-1990_01 |
| ORD ID | ord-f1dfed6d36574850a6245e0f377c767f |
| Quellennotiz | uspto-grants-1990_01 |