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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 330065Erstellt: 24. Oktober 2026

Deferiprone → ZINC 3-hydroxy-1,2-dimethylpyrid-4-one

https://huagongshe.com/de/reaction/330065

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktDeferiproneHCID 2972—
EduktZINC 1-ethyl-3-hydroxypyrid-2-oneHCID 70373874—
LösungsmittelEthanolHCID 702—
ProduktZINC 3-hydroxy-1,2-dimethylpyrid-4-oneHCID 70373691—

Reaktionsschritte

The procedure described under (A) is followed with 3-hydroxy-1,2-dimethylpyrid-4-one in place of 1-ethyl-3-hydroxypyrid-2-one to give the neutral 2:1 complex from ethanol as a white crystalline solid in essentially quantitative yield, m.p. 190° C. (with decomposition); νmax 1655, 1612 cm-1 ; δ(d6DMSO); 7.53 (d, 1H), 6.20 (d, 1H), 3.70 (s, 3H), 2.33 (s, 3H).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04894455
Quelldatensatzuspto-grants-1990_01
ORD IDord-75c709617744441185b11998ecb3a51b
Quellennotizuspto-grants-1990_01