HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl iodide → HCID 178480658, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl iodide | HCID 6328 | — |
| Edukt | 1-(4-Chlorophenyl)-1H-imidazole | HCID 142859 | — |
| Lösungsmittel | Tetrahydrofuran | HCID 8028 | — |
| Produkt | HCID 178480658 | HCID 178480658 | — |
Reaktionsschritte
1-(4-Chlorophenyl)imidazole (0.37 g, 2.07 mmol) is dissolved in THF (5 ml) and subsequently admixed with methyl iodide (1.47 g, 10.4 mmol) and allowed to stand for 20 hours. The precipitate formed is subsequently filtered off and washed with ethanol and with petroleum ether and subsequently dried under reduced pressure. This gives 0.46 g of 1-(4-chlorophenyl)-3-methylimidazolium iodide.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08877937B2 |
| Quelldatensatz | uspto-grants-2014_11 |
| ORD ID | ord-676487415dcd4a69a0c42a1697107604 |
| Quellennotiz | uspto-grants-2014_11 |