Methyl iodide → HCID 178480658, Verbindung

HRID 333020

Reaktionsgleichung

Reaktionsgleichung von HRID 333020
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[CH:11][N:10]=[CH:9]2)=[CH:4][CH:3]=1.[CH3:13][I:14]>C1COCC1>[I-:14].[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([N+:8]2[CH:12]=[CH:11][N:10]([CH3:13])[CH:9]=2)=[CH:6][CH:7]=1

Komponenten

4

Edukt 2

HCID 6328Methyl iodideHCID 1428591-(4-Chlorophenyl)-1H-imidazole

Produkt 1

HCID 178480658HCID 178480658, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 8028TetrahydrofuranLösungsmittel

Versuchsvorschrift

1-(4-Chlorophenyl)imidazole (0.37 g, 2.07 mmol) is dissolved in THF (5 ml) and subsequently admixed with methyl iodide (1.47 g, 10.4 mmol) and allowed to stand for 20 hours. The precipitate formed is subsequently filtered off and washed with ethanol and with petroleum ether and subsequently dried under reduced pressure. This gives 0.46 g of 1-(4-chlorophenyl)-3-methylimidazolium iodide.

Aufarbeitung

  1. customThe precipitate formed
  2. filtrationis subsequently filtered off
  3. washwashed with ethanol and with petroleum ether
  4. customsubsequently dried under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-676487415dcd4a69a0c42a1697107604
Quelldatensatz
uspto-grants-2014_11
Patentnummer
US08877937B2

Verknüpfte Notizen

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