HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-(2,5-Xylyl)piperazine → HCID 71602643, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-(2,5-Xylyl)piperazine | HCID 70542 | — |
| Edukt | (1,1'-Biphenyl)-2-carboxaldehyde | HCID 121052 | — |
| Edukt | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Edukt | 1-(Biphenyl-2-ylmethyl)-4-phenylpiperazine | HCID 71602523 | — |
| Produkt | HCID 71602643 | HCID 71602643 | — |
Reaktionsschritte
35.8 mg of the target compound (0.10 mmol, 12.2%) was obtained using 1-(2,5-dimethylphenyl)piperazine (312 mg, 1.64 mmol), biphenyl-2-carbaldehyde (150 mg, 0.82 mmol) and NaBH(OAc)3 (529 mg, 2.46 mmol) according to the synthesis method of Compound 1.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08883796B2 |
| Quelldatensatz | uspto-grants-2014_11 |
| ORD ID | ord-38b5ab2a6c8044808dcfbdceb29b8215 |
| Quellennotiz | uspto-grants-2014_11 |