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Methylhydrazine → 1-[1-(4-Fluorophenyl)-2-methylsulfonylethylidene]-2-methylhydrazine

HRID 335436
Notizen
Druckvorschau

Reaktionsgleichung

Reaktionsgleichung von HRID 335436
[F:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=O)[CH2:9][S:10]([CH3:13])(=[O:12])=[O:11])=[CH:4][CH:3]=1.[CH3:15][NH:16][NH2:17]>C(O)C>[F:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[N:17][NH:16][CH3:15])[CH2:9][S:10]([CH3:13])(=[O:12])=[O:11])=[CH:4][CH:3]=1
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Komponenten

4

Edukt 2

HCID 6061MethylhydrazineHCID 14882461-(4-Fluorophenyl)-2-(methylsulfonyl)-1-ethanone

Produkt 1

HCID 866893531-[1-(4-Fluorophenyl)-2-methylsulfonylethylidene]-2-methylhydrazineAusbeute 31,9 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 702EthanolLösungsmittel

Versuchsvorschrift

To a 50 ml volume three-necked flask, 1-(4-fluorophenyl)-2-methylsulfonylethan-1-one (7-2-3) (5.0 g), methylhydrazine (14-a) (1.2 g), and ethanol (17.1 ml) were added under a nitrogen atmosphere, and heated to reflux for 4 hours. After the mixture was cooled, the precipitated solid was removed by filtration. The filtrate was concentrated under reduced pressure. To the residue was added hot hexane to be dissolved. The mixture was left to cool. Then, the precipitated crystals were collected by filtration, washed, and dried under reduced pressure. The crystal was purified by recrystallization (methanol) to give 1.8 g of 1-[1-(4-fluorophenyl)-2-methylsulfonylethylidene]-2-methylhydrazine (5-2-4).

Aufarbeitung

  1. temperatureheated
  2. temperatureto reflux for 4 hours
  3. temperatureAfter the mixture was cooled
  4. customthe precipitated solid was removed by filtration
  5. concentrationThe filtrate was concentrated under reduced pressure
  6. additionTo the residue was added hot hexane
  7. dissolutionto be dissolved
  8. waitThe mixture was left
  9. temperatureto cool
  10. filtrationThen, the precipitated crystals were collected by filtration
  11. washwashed
  12. customdried under reduced pressure
  13. customThe crystal was purified by recrystallization (methanol)

Quellen und Nachweise

ORD-Eintrag
ord-d148d772ec7a4c2a9691472ccb15f1a3
Quelldatensatz
uspto-grants-2014_11
DOI
10.6084/m9.figshare.5104873.v1
Patentnummer
US08884010B2

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