ER-35786 → 3,5-Dimethyl-1-hexyn-3-ol

Reaktionsgleichung

C(O)#C[OH:3].[CH3:5][C@H:6]1[C:13](S[C@@H]2CN[C@H]([C@H](O)[C@H]3CNCC3)C2)=C(C(O)=O)N2[C@H:7]1[C@@H:8]([C@H:30](O)[CH3:31])[C:9]2=O.Cl>>[CH3:5][CH:6]([CH2:7][C:8]([OH:3])([C:30]#[CH:31])[CH3:9])[CH3:13]

Komponenten

Edukt 2

HCID 6918311ER-35786

HCID 9942115Acetylene glycol

Produkt 1

HCID 610183,5-Dimethyl-1-hexyn-3-ol

Versuchsvorschrift

For example, any commercially available product may be used for the acetylene diol compound. The commercially available product includes, for example, “Olfin (trade name) E1010” and “Olfin (trade name) E1004” as well as “Surfynol (trade name) 440” and “Surfynol (trade name) 465” produced by Nissin Chemical Industry Co., Ltd.; and “Acetylenol (trade name) E40” and “Acetylenol (trade name) E100” produced by Kawaken Fine Chemicals Co., Ltd.

Quellen und Nachweise

ORD-Eintrag: ord-4e67c40a803348bcaecdf2d7b276d516
Quelldatensatz: uspto-grants-2014_11
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US08889762B2

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