HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Formic Acid → HCID 178420610, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Formic Acid | HCID 284 | — |
| Edukt | Aniline | HCID 6115 | — |
| Edukt | 2,6-Diformylpyridine | HCID 79485 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178420610 | HCID 178420610 | — |
Reaktionsschritte
2,6-pyridine dicarboxaldehyde (0.3071 g, 2.3 mmol) was added to a solution of aniline (0.5292 g, 5.7 mmol) in absolute ethanol (20 mL) at room temperature. 0.5 mL of formic acid was then added to the above solution. The mixture was stirred at room temperature for 65 hours. The product was filtered, washed with cold ethanol and dried in a vacuum oven (50° C.) overnight. Yield 0.2245 g (34.2%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07429684B2 |
| Quelldatensatz | uspto-grants-2008_09 |
| ORD ID | ord-21efaacccac443d7a83aa3e70255ab54 |
| Quellennotiz | uspto-grants-2008_09 |