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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 33818Erstellt: 23. Oktober 2026

Formic Acid → HCID 178420610, Verbindung

https://huagongshe.com/de/reaction/33818

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktFormic AcidHCID 284—
EduktAnilineHCID 6115—
Edukt2,6-DiformylpyridineHCID 79485—
LösungsmittelEthanolHCID 702—
ProduktHCID 178420610HCID 178420610—

Reaktionsschritte

2,6-pyridine dicarboxaldehyde (0.3071 g, 2.3 mmol) was added to a solution of aniline (0.5292 g, 5.7 mmol) in absolute ethanol (20 mL) at room temperature. 0.5 mL of formic acid was then added to the above solution. The mixture was stirred at room temperature for 65 hours. The product was filtered, washed with cold ethanol and dried in a vacuum oven (50° C.) overnight. Yield 0.2245 g (34.2%).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07429684B2
Quelldatensatzuspto-grants-2008_09
ORD IDord-21efaacccac443d7a83aa3e70255ab54
Quellennotizuspto-grants-2008_09