HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Heptanamine → 3-amino-4-hydroxy-N-(1-propylbutyl)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Heptanamine | HCID 38665 | — |
| Edukt | 3-Amino-4-hydroxybenzoic acid | HCID 65083 | — |
| Produkt | 3-amino-4-hydroxy-N-(1-propylbutyl)benzamide | HCID 66773120 | 57% |
Reaktionsschritte
3-amino-4-hydroxy-N-(1-propylbutyl)benzamide was prepared in a similar manner to example 4 using 3-Amino-4-hydroxybenzoic acid and 4-heptylamine. Yield 57%. 1H NMR (500 MHz, CDCl3): δ 0.93 (t, 6H); 1.26-1.51 (m, 8H); 4.09 (m, 1H); 6.74 (m, 1H); 7.05 (s, 1H); 7.43 (m, 2H); 7.77 (m, 2H). MS: (251, M+H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08895050B2 |
| Quelldatensatz | uspto-grants-2014_11 |
| ORD ID | ord-2e3ce0e3ec9140c6a2db21225c34d2f5 |
| Quellennotiz | uspto-grants-2014_11 |