HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Hydroxide → Sodium 6-methoxynicotinate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | Methyl 6-methoxypyridine-3-carboxylate | HCID 586039 | — |
| Lösungsmittel | 1,4-Dioxane | HCID 31275 | — |
| Produkt | Sodium 6-methoxynicotinate | HCID 23717611 | — |
Reaktionsschritte
methyl 6-methoxynicotinate (2.097 g, 12.56 mmol) was dissolved in dioxane (30 mL). An aqueous solution of NaOH (1.0N, 25 mL) was added to the solution and the mixture was stirred at room temperature overnight. The solvent was removed under reduced pressure to provide 2.2 g of sodium 6-methoxynicotinate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08895050B2 |
| Quelldatensatz | uspto-grants-2014_11 |
| ORD ID | ord-0482b300a3214a2a9e2d4a88299a8574 |
| Quellennotiz | uspto-grants-2014_11 |