Sodium Hydroxide → Sodium 6-methoxynicotinate

HRID 339380

Reaktionsgleichung

Reaktionsgleichung von HRID 339380
[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:6]([C:7]([O:9]C)=[O:8])=[CH:5][N:4]=1.[OH-].[Na+:14]>O1CCOCC1>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:6]([C:7]([O-:9])=[O:8])=[CH:5][N:4]=1.[Na+:14]

Komponenten

4

Edukt 2

HCID 14798Sodium HydroxideHCID 586039Methyl 6-methoxypyridine-3-carboxylate

Produkt 1

HCID 23717611Sodium 6-methoxynicotinate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 312751,4-DioxaneLösungsmittel

Versuchsvorschrift

methyl 6-methoxynicotinate (2.097 g, 12.56 mmol) was dissolved in dioxane (30 mL). An aqueous solution of NaOH (1.0N, 25 mL) was added to the solution and the mixture was stirred at room temperature overnight. The solvent was removed under reduced pressure to provide 2.2 g of sodium 6-methoxynicotinate.

Aufarbeitung

  1. customThe solvent was removed under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-0482b300a3214a2a9e2d4a88299a8574
Quelldatensatz
uspto-grants-2014_11
Patentnummer
US08895050B2

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