HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-(6-Methoxy-1,3-benzothiazol-2-yl)aniline → HCID 67313154, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-(6-Methoxy-1,3-benzothiazol-2-yl)aniline | HCID 391870 | — |
| Edukt | 4-Methoxy-3-(trifluoromethyl)benzoyl chloride | HCID 2775298 | — |
| Lösungsmittel | Pyridine | HCID 1049 | — |
| Produkt | HCID 67313154 | HCID 67313154 | 87% |
Reaktionsschritte
Prepared as described in the Amide Coupling section using 2-(4-aminophenyl)-6-methoxybenzothiazole (0.5 g, 1.95 mmol) and 4-methoxy-3-trifluoromethylbenzoyl chloride (0.47 g, 1.95 mmol) in dry pyridine (15 ml) to give the title compound (0.77 g, 87%) as pale yellow feathery crystals after work-up and recrystallisation from acetic acid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08895313B2 |
| Quelldatensatz | uspto-grants-2014_11 |
| ORD ID | ord-f231a315b48e409ca85777f2f217b6a9 |
| Quellennotiz | uspto-grants-2014_11 |