HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 339839Erstellt: 24. Oktober 2026
Tetramethyl orthocarbonate → 5-(3-Bromophenyl)-2-methoxy-6,6-dimethyl-5,6-dihydro-1,4,3-oxathiazine 4,4-dioxide
https://huagongshe.com/de/reaction/339839
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Tetramethyl orthocarbonate | HCID 74613 | — |
| Edukt | 1-(3-Bromophenyl)-2-hydroxy-2-methylpropane-1-sulfonamide | HCID 68291860 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | 5-(3-Bromophenyl)-2-methoxy-6,6-dimethyl-5,6-dihydro-1,4,3-oxathiazine 4,4-dioxide | HCID 68359202 | — |
Reaktionsschritte
A mixture of 500 mg of 1-(3-bromophenyl)-2-hydroxy-2-methylpropane-1-sulfonamide in 2 ml of tetramethoxymethane and 0.5 ml of acetic acid was stirred at 100° C. for 3 hours. After the removal of the solvent under reduced pressure, the residue (565 mg) was used in the next reaction without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US08895547B2 |
|---|
| Quelldatensatz | uspto-grants-2014_11 |
|---|
| ORD ID | ord-da8c1461b04e494cb05814fd65140e10 |
|---|
| Quellennotiz | uspto-grants-2014_11 |
|---|
