Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Tetraethyl orthocarbonate | HCID 66213 | — |
| Edukt | Biphenyl-4-yl-(3-hydroxyoxetan-3-yl)methanesulfonamide | HCID 68359244 | — |
| Lösungsmittel | Acetic Acid | HCID 176 | — |
| Produkt | HCID 68292566 | HCID 68292566 | — |
Reaktionsschritte
A mixture of 0.17 g of biphenyl-4-yl-(3-hydroxyoxetan-3-yl)methanesulfonamide in 4 ml of tetraethoxymethane and 1 ml of acetic acid was stirred at 90° C. for 3 hours. The solvent was removed under reduced pressure. This gave the crude product, which was used without further purification.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US08895547B2 |
|---|
| Quelldatensatz | uspto-grants-2014_11 |
|---|
| ORD ID | ord-c6b9c90066244e549bc33fd27109c190 |
|---|
| Quellennotiz | uspto-grants-2014_11 |
|---|
