HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 340462Erstellt: 23. Oktober 2026
Dimethylformamide dimethyl acetal → 1-(5-Bromopyridin-3-yl)-3-(dimethylamino)prop-2-ene-1-one
https://huagongshe.com/de/reaction/340462
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Edukt | 3-Acetyl-5-bromopyridine | HCID 820423 | — |
| Produkt | 1-(5-Bromopyridin-3-yl)-3-(dimethylamino)prop-2-ene-1-one | HCID 67057279 | — |
Reaktionsschritte
An N,N-dimethylformamide dimethylacetal (2 ml) solution containing 1-(5-bromopyridin-3-yl)ethanone (100 mg) (WO2009/87224 A1) was stirred at 100° C. for 5 hours. The solvent was distilled away under reduced pressure, and a yellow solid of 1-(5-bromopyridin-3-yl)-3-(dimethylamino)prop-2-ene-1-one was thus obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US08895585B2 |
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| Quelldatensatz | uspto-grants-2014_11 |
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| ORD ID | ord-9ea3052c2c8641589f76c41843130f54 |
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| Quellennotiz | uspto-grants-2014_11 |
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