Thionyl Chloride → 3-(Chlorocarbonyl)phenyl acetate

Beteiligte Stoffe

Reaktionsschritte

Using the above procedure, reaction of with thionyl chloride (11.1 mL, 15.3 mmol) and 3-acetoxybenzoic acid (2.50 g, 13.9 mmol) gave 511 (2.72 g, 99%) as a colorless oil. This material was used in the next step without additional purification.

Herkunft & Nachweise