HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Potassium Hydroxide → 1-Methyl-1H-indole-6-carboxylic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | 1-Methyl-1H-indole-6-carbonitrile | HCID 15384493 | — |
| Edukt | Water ethanol | HCID 19096565 | — |
| Produkt | 1-Methyl-1H-indole-6-carboxylic acid | HCID 19819261 | — |
Reaktionsschritte
1-Methyl-6-cyanoindole (3.12 g, 21.9 mmole) was heated at reflux in 180 mL of ethanol/water (8:1) containing 15 g of potassium hydroxide to give 3.0 g of 1-methyl-1H-indole-6-carboxylic acid as a white solid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05856517 |
| Quelldatensatz | uspto-grants-1999_01 |
| ORD ID | ord-17aa20e8fd2440d188bd859f149319d1 |
| Quellennotiz | uspto-grants-1999_01 |