HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Formic Acid → 2,6-Naphthalene dicarboxylic acid copper
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Formic Acid | HCID 284 | — |
| Edukt | 2,6-Naphthalenedicarboxylic acid | HCID 14357 | — |
| Edukt | Formic acid, copper salt | HCID 44152240 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 2,6-Naphthalene dicarboxylic acid copper | HCID 69858079 | 67,6% |
Reaktionsschritte
0.40 g of 2,6-naphthalene dicarboxylic acid was dissolved under heating in a mixture solvent of 4000 cm3 of methanol and 5 cm3 of formic acid. After this solution was cooled to the normal temperature, into this solution under stirring, a further solution in which 3.00 g of formic acid copper was dissolved in 100 cm3 of methanol was dripped and then this was kept still for a few days. Thereafter, the precipitation product was suction-filtered and dried for 110° C./4 hours, whereby 0.35 g of 2,6-naphthalene dicarboxylic acid copper was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05862796 |
| Quelldatensatz | uspto-grants-1999_01 |
| ORD ID | ord-c4bbc6cb1fc74cb0907db7ff81c62b12 |
| Quellennotiz | uspto-grants-1999_01 |