Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Calcium Carbonate | HCID 10112 | — |
| Edukt | 3-(1-Bromoethyl)benzophenone | HCID 12802924 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 3-(1-Hydroxyethyl)benzophenone | HCID 13102751 | — |
Reaktionsschritte
In an autoclave, 100 ml of water and 3.3 g of calcium carbonate and 10 g of 3-(1-bromoethyl)benzophenone were placed, and were then heated at 120° C. for 6 hours. The resultant reaction solution was extracted with benzene, and a formed benzene layer was then dried with anhydrous sodium sulfate, followed by distilling off the solvent. The resultant product had the spectrum data which were identical with those of 3-(1-hydroxyethyl)benzophenone.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US04761508 |
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| Quelldatensatz | uspto-grants-1988_08 |
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| ORD ID | ord-fc7d2b8db3824fb2971244479323f773 |
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| Quellennotiz | uspto-grants-1988_08 |
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