HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Diethyl Ether → 9-Octadecenal, (9Z)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Diethyl Ether | HCID 3283 | — |
| Edukt | Oleyl Alcohol | HCID 5284499 | — |
| Edukt | HCID 178418287 | HCID 178418287 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 9-Octadecenal, (9Z)- | HCID 5364492 | 90,1% |
Reaktionsschritte
An 18 g portion of pyridinium chlorochromate was slurried in 200 ml of dichloromethane. A solution of 15 g of oleyl alcohol in 200 ml of dichloromethane was added. This mixture was stirred for 4 hours, then poured into ether and filtered through hydrous magnesium silicate. The filtrate was evaporated, giving 13.42 g of the desired compound as a colorless liquid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05053426 |
| Quelldatensatz | uspto-grants-1991_10 |
| ORD ID | ord-0a27b92f0b3f46f8b3c80fea1702af49 |
| Quellennotiz | uspto-grants-1991_10 |