HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Adamantanol → 1-Adamantyl 2-(p-nitrophenyl)propionate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Adamantanol | HCID 64152 | — |
| Edukt | 2-(4-Nitrophenyl)propionic acid | HCID 89244 | — |
| Edukt | 1-Methylcyclohexyl 2-(p-nitrophenyl)propionate | HCID 54068492 | — |
| Produkt | 1-Adamantyl 2-(p-nitrophenyl)propionate | HCID 21298167 | 92% |
Reaktionsschritte
Using a method similar to that used in the preparation of 1-methylcyclohexyl 2-(p-nitrophenyl)propionate, 14.6 g of 2-(p-nitrophenyl)propionic acid, but using 1-adamantol instead of 1-methylcyclohexanol, were reacted to obtain 22.74 g (92% yield) of 1-adamantyl 2-(p-nitrophenyl)propionate as a light yellow viscous liquid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04762840 |
| Quelldatensatz | uspto-grants-1988_08 |
| ORD ID | ord-c5b67b715fb843d8baa6939c205a5268 |
| Quellennotiz | uspto-grants-1988_08 |