Piperidin-2-ylmethanol → N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-2-hydroxymethylpiperidine

HRID 34566

Reaktionsgleichung

Reaktionsgleichung von HRID 34566
[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([OH:6])=O.[OH:23][CH2:24][CH:25]1[CH2:30][CH2:29][CH2:28][CH2:27][NH:26]1>>[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([N:26]1[CH2:27][CH2:28][CH2:29][CH2:30][CH:25]1[CH2:24][OH:23])=[O:6]

Komponenten

3

Edukt 2

HCID 94263Piperidin-2-ylmethanolHCID 1285703,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenic acid

Produkt 1

HCID 53831595N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-2-hydroxymethylpiperidineAusbeute 94 %

Versuchsvorschrift

The procedure of Example 1 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid and 3.5 g of 2-hydroxymethylpiperidine were used as starting materials. 7.5 g (yield 94%) of the title compound was obtained as a colorless oil.

Quellen und Nachweise

ORD-Eintrag
ord-93e161664f034de6b88afd36a2870e93
Quelldatensatz
uspto-grants-1988_08
Patentnummer
US04762829

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