HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Tridecanoic acid → Tridecanoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Tridecanoic acid | HCID 12530 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | Tridecanoyl chloride | HCID 87288 | — |
Reaktionsschritte
To a benzene solution containing 5.0 g (0.023 mol) of tridecanoic acid was added 25 g of thionyl chloride, followed by refluxing for 5 hours. The excess of thionyl chloride and benzene were removed by distillation to obtain tridecanoyl chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05059628 |
| Quelldatensatz | uspto-grants-1991_10 |
| ORD ID | ord-b6fd7f8ab8d244baa08dccc98c1036ee |
| Quellennotiz | uspto-grants-1991_10 |