HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Pyrrolidine → BOC-L-methionyl-pyrrolidine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Pyrrolidine | HCID 31268 | — |
| Edukt | Boc-L-methionine | HCID 89857 | — |
| Produkt | BOC-L-methionyl-pyrrolidine | HCID 11034003 | — |
Reaktionsschritte
2.50 g (10 mmol) BOC-methionine was coupled to 1.72 ml (20.6 mmol) pyrrolidine according to procedure B. Yield of crude product 3.38 g. The product was purified with a silica column using ethyl acetate as eluent. Yield 2.81 g (9.3 mmol, 93%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07173024B2 |
| Quelldatensatz | uspto-grants-2007_02 |
| ORD ID | ord-b0b858eef19d47ada090bbefcb651833 |
| Quellennotiz | uspto-grants-2007_02 |