HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium Carbonate → HCID 16119014, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium Carbonate | HCID 10340 | — |
| Edukt | m-Fluorobenzenethiol | HCID 75710 | — |
| Edukt | HCID 86595861 | HCID 86595861 | — |
| Lösungsmittel | Acetonitrile | HCID 6342 | — |
| Produkt | HCID 16119014 | HCID 16119014 | — |
Reaktionsschritte
(R)-2-(5-{[(3-chloro-2-methylphenyl)sulfonyl]amino}-1,2,4-thiadiazol-3-yl)-1-methylethyl 3-chloro-2-methylbenzenesulfonate (example 98), 3-fluorothiophenol (1 eq) and sodium carbonate (1 eq) in CH3CN were heated overnight. Standard work-up and purification yielded the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07173030B2 |
| Quelldatensatz | uspto-grants-2007_02 |
| ORD ID | ord-b45a8fbabee84cd3a770253cd1beedb7 |
| Quellennotiz | uspto-grants-2007_02 |